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A crucible with a coal sample weighted 9.2710 g after heating at 108 0C for 1hr and coal sample analyzed for having 30% of moisture. This sample was further heated at 920 0C in crucible with lid for 7 min and then without lid at 750 0C and weighted 9.2131 g and 8.8758 g respectively. Finally, 0.3102 g of ash was washed off from the crucible for further use. Give a proximate analysis of given coal sample

Question

A crucible with a coal sample weighted 9.2710 g after heating at 108 0C for 1hr and coal sample analyzed for having 30% of moisture. This sample was further heated at 920 0C in crucible with lid for 7 min and then without lid at 750 0C and weighted 9.2131 g and 8.8758 g respectively. Finally, 0.3102 g of ash was washed off from the crucible for further use. Give a proximate analysis of given coal sample

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Solution

The proximate analysis of a coal sample involves the determination of various components of coal, such as moisture, volatile matter, fixed carbon, and ash.

  1. Moisture Content: The moisture content is given as 30%.

  2. Volatile Matter: This is calculated by subtracting the weight of the sample after heating at 920°C with the lid on from the initial weight of the sample, then dividing by the initial weight and multiplying by 100.

    (9.2710 g - 9.2131 g) / 9.2710 g * 100 = 0.625%

  3. Fixed Carbon: This is calculated by subtracting the weight of the sample after heating at 750°C without the lid from the weight of the sample after heating at 920°C with the lid on, then dividing by the initial weight and multiplying by 100.

    (9.2131 g - 8.8758 g) / 9.2710 g * 100 = 3.64%

  4. Ash Content: This is calculated by dividing the weight of the ash by the initial weight of the sample and multiplying by 100.

    0.3102 g / 9.2710 g * 100 = 3.34%

So, the proximate analysis of the coal sample is:

  • Moisture: 30%
  • Volatile Matter: 0.625%
  • Fixed Carbon: 3.64%
  • Ash: 3.34%

Please note that these values are approximate and actual values may vary depending on the specific conditions of the experiment.

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